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alkaloids, to unreacted lysergic acid, or lysergic acid hydrazides to iso-
LSD and God knows what substances created by the mishandling of
the raw materials and product, a contaminated product is much easier to
make than a pure one.
The use of large volumes of solvents poses twin problems:
obtaining them and disposing of them. Both problems are made vastly
Practical LSD Manufacture
simpler by recycling the solvents. Just because a solvent has been
used once in a given stage of the process does not mean its useful
lifetime is over. For example, the solvent used for defatting the crop is
easily made as good as new by distilling it to free it of its load of fat.
Other solvents are not so easily recovered for re-use because the
procedure calls for the given solvent to be removed from the product
by vacuum evaporation. In this case, the solvent can be collected in a
cold trap placed along the vacuum line on its way to the vacuum
source. If a pump is used to create the vacuum, such a trap is vital to
prevent solvent vapors from getting into the pump oil, thereby ruining
the lubrication and the vacuum created.
A cold trap can be constructed of either glass or steel; it need only be
large enough to hold the solvent collected, and airtight so as not to ruin
the vacuum with leaks. This cold trap is then cooled down with dry ice
during vacuum evaporations to condense the solvent vapors in the trap.
The solvent recovered in the trap can be re-used in the given stage of
the process from whence it came. I would not co-mingle recovered
solvents from different stages. For example, chloroform from the
alkaloid extraction of the crops should be kept for that usage, and not
be used for LSD crystallization, because it will also contain some
ammonia and methanol.
The recovery of ether, for example, from method 2 of lysergic acid
production, poses a special problem. This problem is the formation of
explosive peroxides in ether during storage. Ether containing water
and alcohol, as would be the case for this recovered solvent, does not
form much peroxide.
There is a possibility that dry ether can be made
free of peroxides by shaking the ether with some 5% ferrous sulfate
(FeSO4) solution in water prior to distilling.
Failure to do this may
expose the operator to a fiery explosion during distillation.
flowing through the condenser, and an ice-chilled receiving flask, are
required to get an efficient condensation of the ether during
Keeping Out Of Trouble 71
Keeping Out Of Trouble
The dangers of Damianadopamine
LSD manufacturing do not end with the possibility
that the cooker may spill some of the stuff on himself and fry his
brain. There is a much more malignant danger facing those who
embark upon this course: Johnny Law.
The conduit through which those shit-eating dogs travel to get to
you is your associates. If you are cooking alone with no partners in
crime, your safety has been impro
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w. Case in point is the hydriodic acid and red phosphorus reduction of
ephedrine to methamphetamine. If in this reaction the ephedrine is not
fairly free of the fillers and binders found in the stimulant pills from
which it is extracted, the result at the end of the reaction is a heavy
reduction in the yield of product, and the formation of a most stubborn
emulsion from which the desired meth is extracted only with
LSD Production: An Overview
great difficulty. This is the origin of the revolting peanut butter
consistency of most meth seen on the market. Similarly, one can only
expect success in the production of high-grade LSD if care is taken
throughout the procedure to ensure that the materials used meet the
requirement of a reasonable degree of purity.
The actual synthesis of LSD is an exquisite combination of
farming skills, biology, biochemistry and organic chemistry. In its
preferred embodiment, a scheme for the large-scale manufacture of
LSD would center around someone playing weekend hobby farmer on an
acre or two of land. On this land, our happier-than-most farmer
would plant either rye to be infested with the Claviceps fungus to
produce a crop of ergot; morning glories for the eventual harvest of
their seeds; or, if local weather conditions permit, Hawaiian baby
woodrose, also for the harvest of its seeds.
Mother Nature's bounty is then squirreled off to the lab site for
the biochemical phase of the process — the isolation of the lysergic
alkaloids. Here one or more of a series of alkaloids are freed from the
very complex plant matrix and hopefully isolated in a pure form.
These alkaloids all have one thing in common — they are amides of
lysergic acid. See the structures of the major naturally occurring
amides pictured below:
Practical LSD Manufacture
They all contain the lysergic acid molecule shown below:
The lysergic acid molecule is the key to all known methods of
LSD production. The common thread that all the synthetic routes to
LSD share is that the path they travel starts with the naturally
occurring alkaloids, the amide linkage is lopped off to give lysergic
acid, and then the lysergic acid is reacted with diethylamine to give
LSD shown below:
The nuts and bolts of how this is done will be explained in the
2 Sources Of The Lysergic Amides
Sources Of The
Let me begin this chapter by nuking an oft-chanted mantra, this
mantra being the claim that a person can grow ergot fungus in a
culture medium and get it to produce lysergic acid amides to feed into
LSD production. This claim as seen in Psychedelic Chemistry and
other publications I read while in college is pure BS. It is truly
unfortunate that nature does not cooperate in this manner, since this
would obviously be the best way to set up a large-scale production
operation, as the logistical complications of crop growth and harvest
would then be eliminated.
Let me give a science and lit
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