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nt a bunch of
thallium around the house about like you want to be kicked in the
teeth with a heavy pair of boots.
A further bad aspect of this method is its high cost. 100 grams sell
for $150, and the high molecular weight of the compound means that a
lot of it has to be used to get a moderate amount of product. One
pound of thallium(ni) nitrate is required for a 1-molar batch.
This method can be found in Tetrahedron Letters No. 60, pages
5275-80 (1970). To produce a one mole batch, dissolve one mole of
propenylbenzene in some methanol, and put it into a one-gallon glass
jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate
trihydrate in methanol. Then pour the thallium solution into the jug
with the propenylbenzene, and stir at room temperature for 5 minutes.
The thallium(I) nitrate formed by the reaction comes out of solution. It is
removed by filtration.
The propenylbenzene has at this point been converted to a ketal.
This is hydrolyzed to the phenylacetone by shaking the filtrate with
about 2000 ml of 1 molar sulfuric acid solution in water for about 5
minutes. The phenylacetone is then extracted out with a couple of
portions of tolulene. This extract is then washed with 5% NaOH
solution, then distilled or purified by conversion to the bisulfite
12 Studies On The Production OfTMA-2
Production of TMA-2, MDA, etc. from the
There are three good methods for converting the phenylacetone to
the psychedelic amphetamine. Choice number one is to use reductive
amination with a hydrogenation bomb with Raney nickel, ammonia
and alcohol solvent. See Journal of the American Chemical Society,
Volume 70, pages 12811-12 (1948). Also see Chem. Abstracts from
1954, column 2097. This gives a yield of about 80% if plenty of
Raney nickel is used. The preferred conditions for use with MDA is a
temperature of 80 C, and a hydrogen pressure of 50 atmospheres.
The drawback to this method is the need for a shaker device for
the bomb, and also a heater. The use of platinum as the catalyst in the
bomb works great when making MDMA, but gives lousy results when
making MDA. There may be a way around this, however, for serious
experimenters. It has been found in experiments with phenylacetone
that a mixture of ammonia and ammonium chloride produces good
yields of amphetamine (50%) when used in a bomb with platinum
catalyst. Methylenedioxyphenylacetone is quite likely to behave
similarly, along with other phenylacetones.
To use this variation, the following materials are placed in the 1.5
liter champagne bottle hydrogenation device described in Chapter 11 of
Secrets of Methamphetamine Manufacture, Third Edition: .5 gram
platinum in 20 ml distilled water. If this platinum is in the form of
PtO2 instead of reduced platinum metal catalyst obtained with
borohydride, the experimenter must now reduce the platinum by
pressurizing the bottle with hydrogen and stirring fo
ayahuasca school Recreational Hallucinogenic Frogs For Sale
hallucinogenic frog for sale there is decent drainage.
Cacti tend to grow mostly during spring and autumn, to send down roots in the
summer, and to rest through winter.
Although cactus cuttings may be planted anytime of the year they stand the best chance if planted in the late spring. They should be watered thoroughly once or twice a week depending upon how rapidly moisture is lost. The soil an inch below the surface should always contain some moisture. Watering can be cut back to less than half during the winter. INCREASING THE POTENCY OF PSYCHOACTIVE CACTI There are several factors which influence production of mescaline and related alkaloids in cacti. Presence of a wide variety of trace minerals is important. Occasional watering with Hoagland A-Z trace mineral concentrate provides these minerals. Combine 1 part concentrate with 9 parts water and water cacti with this once every two months. Experiments conducted by Rosenberg, Mclaughlin and Paul at the University of of Michigan, Ann Arbor in 1966 demonstrated that dopamine is a precursor of mescaline in the peyote cactus.
Tyramine and dopa were also found to be mescaline precursors, but not as immediate and efficient as dopamine. It appears that in the plant tyosine breaks down to become tyramine and dopa. These then recombine to form dopamine which is converted to nor-mescaline and finally to mescaline. One can take advantage to this sequence by inject-ing each peyote plant with dopamine 4 weeks prior to harvesting.
Much of the dopamine will convert to mescaline during this time, giving a considerable increase in the alkaloid of the plant. Prepare a saturated solution of free base dopamine in a .05 N solution of hydrochloric acid and inject 1-2 cc into the root of each plant and the same amount into the green portion above the root. Let the needle penetrate to the center of the plant, inject slowly and allow the needle to remain in place a few seconds after injection. It is best to deprive the plant of water for 1-2 weeks before injection. This makes the plant tissues take up the injection fluids more readily. If dopamine is not available, a mixture of tyramine and dopa can be used instead 6 weeks before harvesting for comparable results.
San Pedro and other mescaline-bearing cacti can be similarly treated for increased mescaline production. Inject at the base of the plant and again every 3-4 inches following a spiral pattern up the length of the plant. A
hallucinogenic frog for saleseries of booster injections can be given to any of these cacti every 6-8 weeks and once again 4 weeks before harvesting for greater mescaline accumulation. It is also possible to increase the macromerine and nor-macromerine content of Doñana cacti using tyramine or DL-norepinephrine as precursors. Injections should be given 20-25 days before harvesting. Series of injections can be given 45 days apart for higher alkaloid accumulation.
EXTRACTING PURE MESCALINE FROM PEYOTE OR SAN PEDRO CACTUS The isolation of mescaline from cacti Ayahuasca Recreational