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To make the bisulfite addition product, take the residue from the filtering flask, dissolved in some toluene and freed from catalyst as described above, and pour it in a beaker. Next, add 3 volumes of sodium bisulfite solution prepared by adding sodium bisulfite or metabisulfite to water until no more dissolves. Shake or vigorously stir for a couple of hours to convert the phenylacetone to the solid bisulfite addition product. Filter out the solid, then regenerate pure phenylacetone by putting the solid into a round-bottom flask, adding an excess of saturated solution of sodium bicarbonate in water, and refluxing for a couple hours. After cooling, the phenylacetone should be extracted out with some toluene. The toluene should then be removed under a vacuum, and the residue stored in a freezer until conversion to the amphetamine. All Practical LSD Manufacture 84 phenylacetones are sensitive to light, and should be stored in the freezer. The above cooking procedure is the best way to process allylbenzenes to the corresponding phenylacetones. Sassafras oil, as previously mentioned, is 80-90% safrole. Calumus oil, if its country of origin is India, consists of about 80% of the allyl isomer of asarone: It too can be purified by distillation under a vacuum to yield fairly pure allyl-asarone. Its boiling point is 296° C at normal pressure and about 170° C with aspirator vacuum. More details on this Indian calamus oil can be found in Chetn. Abstracts column 6585 (1935), also Current Science, Volume 3, page 552 (1935). My search for calamus oil of Indian origin came up empty. In fact, the health-food store in my town, which is well-stocked with various oils for use in aromatherapy, had never heard of the stuff, nor was it listed for sale in their catalogs. This left one alternative: dig up the roots of North American calamus, and steam-distill the oil out of them. While searching for calamus in my area's swamps, bogs and ponds, the damaging effects of the spread of purple loosestrife was obvious. This imported plant from Europe has taken over much of the former habitat of the calamus plant. Here in America, the loosestrife is free from the insect that keeps it under control in Europe by feeding on its seeds. The state paper-pushers have been thinking for years about importing the bug, without ever getting off their butts and doing it. I suggest this project to somebody out there in the reading public so that it can finally get done while there is still some native flora left. After a lot of searching, I finally found a large patch of the American calamus. (See Figure 4.) The time for harvesting the roots of the calamus is in the fall after the killing frost. The frost brings the oil down out of the leaves and 12 Studies On The Production OfTMA-2 into the root for winter storage. 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