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nt a bunch of
thallium around the house about like you want to be kicked in the
teeth with a heavy pair of boots.
A further bad aspect of this method is its high cost. 100 grams sell
for $150, and the high molecular weight of the compound means that a
lot of it has to be used to get a moderate amount of product. One
pound of thallium(ni) nitrate is required for a 1-molar batch.
This method can be found in Tetrahedron Letters No. 60, pages
5275-80 (1970). To produce a one mole batch, dissolve one mole of
propenylbenzene in some methanol, and put it into a one-gallon glass
jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate
trihydrate in methanol. Then pour the thallium solution into the jug
with the propenylbenzene, and stir at room temperature for 5 minutes.
The thallium(I) nitrate formed by the reaction comes out of solution. It is
removed by filtration.
The propenylbenzene has at this point been converted to a ketal.
This is hydrolyzed to the phenylacetone by shaking the filtrate with
about 2000 ml of 1 molar sulfuric acid solution in water for about 5
minutes. The phenylacetone is then extracted out with a couple of
portions of tolulene. This extract is then washed with 5% NaOH
solution, then distilled or purified by conversion to the bisulfite
12 Studies On The Production OfTMA-2
Production of TMA-2, MDA, etc. from the
There are three good methods for converting the phenylacetone to
the psychedelic amphetamine. Choice number one is to use reductive
amination with a hydrogenation bomb with Raney nickel, ammonia
and alcohol solvent. See Journal of the American Chemical Society,
Volume 70, pages 12811-12 (1948). Also see Chem. Abstracts from
1954, column 2097. This gives a yield of about 80% if plenty of
Raney nickel is used. The preferred conditions for use with MDA is a
temperature of 80 C, and a hydrogen pressure of 50 atmospheres.
The drawback to this method is the need for a shaker device for
the bomb, and also a heater. The use of platinum as the catalyst in the
bomb works great when making MDMA, but gives lousy results when
making MDA. There may be a way around this, however, for serious
experimenters. It has been found in experiments with phenylacetone
that a mixture of ammonia and ammonium chloride produces good
yields of amphetamine (50%) when used in a bomb with platinum
catalyst. Methylenedioxyphenylacetone is quite likely to behave
similarly, along with other phenylacetones.
To use this variation, the following materials are placed in the 1.5
liter champagne bottle hydrogenation device described in Chapter 11 of
Secrets of Methamphetamine Manufacture, Third Edition: .5 gram
platinum in 20 ml distilled water. If this platinum is in the form of
PtO2 instead of reduced platinum metal catalyst obtained with
borohydride, the experimenter must now reduce the platinum by
pressurizing the bottle with hydrogen and stirring fo school school Peganum Harmala Seeds Spore
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e mental discipline. People who cannot endure the
bitterness of peyote often go to various extremes to get it into the system without
having to taste it. One fairly effective method is to drink unsweetened grapefruit
juice while chewing it. The acids in the juice somewhat neutralize some of the
bitter bases. Another method is to grind the dried buttons in a pepper grinder and
pack the pulverised material into OOO capsules which are washed down with
warm water. This is an effective method but it can take 20 capsules or more to
get a 350mg dose of mescaline. Often people will boil the buttons in water for
several hours to make a concentrated tea. A cup of this decoction
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swallowed in a few hasty gulps. Another preparation that is occasionally used is
a jello-type dessert made with the fresh or dried plant. If spoonfulls are
swallowed whole the gelatine serves as a sort of shield protecting the tastebuds
from contact with the bitter material. It also slows down the the absorption of the
drug in the digestive tract. This can be of value. It is generally recommended that
anyone consuming peyote or mescaline ingest it gradually during a period of an
hour or take two half doses 45 minutes apart. This is done to reduce the shock of
the alkaloid to the system.
Nausea or queasiness is sometimes experienced half
an hour or so after taking peyote or mescaline.
This usually passes in less than
an hour. A sip of grapefruit juice will sometimes dispel the sick feeling. During the
peyote ceremony Indians encourage vomiting rather than restraint if the urge
presents itself. Throwing up, they believe, is apurging of both physical and
spiritual ills. Most tribes fast for at least a day before taking peyote. This can also
help to minimize gastric distress.
One should not have eaten for at least 6 hours
before taking either mescaline or peyote.
A method which avoids both the bitterness and the nausea is the rectal infusion.
8-16 grams of dried peyote is ground
San Pedro Cactus (Trichocereus pachanoi)De-cored Dried Outer Skin into a fine powder and boiled in a pint of
water for 30 minutes. It is then strained and further boiled to reduce it's volume to
one half pint. After cooling, this is taken as an enema using a small bulb syringe
and retained for at least two hours. If there is any fecal matter in the lower bowel,
a small cleansing enema should be taken and thoroughly expelled before having
the peyote infusion. Otherwise much of the drug will be taken up by the feces
and later voided.
FINDING AND PICKING PEYOTE
The peyote cactus may be found in many areas throughout the Chihuahuan
Desert from central Mexico to southern Texas. When a site is found where
peyote grows it usually does so in abundance. Sometimes it grows in open sunlit
places, but more often it is found in clusters under fairly large shrubs, among
mesquite or creosote bushes or in the shade of large succulents.
The best time to harvest any cactus is after a long dry spell.
The worst time is
during or after a rainy period.
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