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alkaloids, to unreacted lysergic acid, or lysergic acid hydrazides to iso-
LSD and God knows what substances created by the mishandling of
the raw materials and product, a contaminated product is much easier to
make than a pure one.
The use of large volumes of solvents poses twin problems:
obtaining them and disposing of them. Both problems are made vastly
Practical LSD Manufacture
simpler by recycling the solvents. Just because a solvent has been
used once in a given stage of the process does not mean its useful
lifetime is over. For example, the solvent used for defatting the crop is
easily made as good as new by distilling it to free it of its load of fat.
Other solvents are not so easily recovered for re-use because the
procedure calls for the given solvent to be removed from the product
by vacuum evaporation.
In this case, the solvent can be collected in a
cold trap placed along the vacuum line on its way to the vacuum
source. If a pump is used to create the vacuum, such a trap is vital to
prevent solvent vapors from getting into the pump oil, thereby ruining
the lubrication and the vacuum created.
A cold trap can be constructed of either glass or steel; it need only be
large enough to hold the solvent collected, and airtight so as not to ruin
the vacuum with leaks. This cold trap is then cooled down
with dry ice
during vacuum evaporations to condense the solvent vapors in the trap.
The solvent recovered
in the trap can be re-used in the given stage of
the process from whence it came. I would not co-mingle recovered
solvents from different stages. For example, chloroform from the
alkaloid extraction of the crops should be kept for that usage, and not
be used for LSD crystallization, because it will also contain some
ammonia and methanol.
The recovery of ether,
for example, from method 2 of lysergic acid
production, poses a special problem. This problem is the formation of
explosive peroxides in ether during storage. Ether containing water
and alcohol, as would be the case for this recovered solvent, does not
form much peroxide. There is a possibility that dry ether can be made
free of peroxides by shaking the ether with some 5% ferrous sulfate
(FeSO4) solution in water prior to distilling.
Failure to do this may
expose the operator to a fiery explosion during distillation.
flowing through the condenser, and an ice-chilled receiving flask, are
required to get an efficient condensation of the ether during
Keeping Out Of Trouble 71
Keeping Out Of Trouble
The dangers of LSD manufacturing do not end with the possibility
that the cooker may spill some of the stuff on himself and fry his
brain. There is a much more malignant danger facing those who
embark upon this course: Johnny Law.
The conduit through which those shit-eating dogs travel to get to
you is your associates. If you are cooking alone with no partners in
crime, your safety has been impro
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@Wednesday, December 19, 2018 4:14:52 PM