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nt a bunch of
thallium around the house about like you want to be kicked in the
teeth with a heavy pair of boots.
A further bad aspect of this method is its high cost. 100 grams sell
for $150, and the high molecular weight of the compound means that a
lot of it has to be used to get a moderate amount of product. One
pound of thallium(ni) nitrate is required for a 1-molar batch.
This method can be found in Tetrahedron Letters No. 60, pages
5275-80 (1970). To produce a one mole batch, dissolve one mole of
propenylbenzene in some methanol, and put it into a one-gallon glass
jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate
trihydrate in methanol. Then pour the thallium solution into the jug
with the propenylbenzene, and stir at room temperature for 5 minutes.
The thallium(I) nitrate formed by the reaction comes out of solution. It is
removed by filtration.
The propenylbenzene has at this point been converted to a ketal.
This is hydrolyzed to the phenylacetone by shaking the filtrate with
about 2000 ml of 1 molar sulfuric acid solution in water for about 5
minutes. The phenylacetone is then extracted out with a couple of
portions of tolulene. This extract is then washed with 5% NaOH
solution, then distilled or purified by conversion to the bisulfite
12 Studies On The Production OfTMA-2
Production of TMA-2, MDA, etc. from the
There are three good methods for converting the phenylacetone to
the psychedelic amphetamine. Choice number one is to use reductive
amination with a hydrogenation bomb with Raney nickel, ammonia
and alcohol solvent. See Journal of the American Chemical Society,
Volume 70, pages 12811-12 (1948). Also see Chem. Abstracts from
1954, column 2097. This gives a yield of about 80% if plenty of
Raney nickel is used. The preferred conditions for use with MDA is a
temperature of 80 C, and a hydrogen pressure of 50 atmospheres.
The drawback to this method is the need for a shaker device for
the bomb, and also a heater. The use of platinum as the catalyst in the
bomb works great when making MDMA, but gives lousy results when
making MDA. There may be a way around this, however, for serious
experimenters. It has been found in experiments with phenylacetone
that a mixture of ammonia and ammonium chloride produces good
yields of amphetamine (50%) when used in a bomb with platinum
catalyst. Methylenedioxyphenylacetone is quite likely to behave
similarly, along with other phenylacetones.
To use this variation, the following materials are placed in the 1.5
liter champagne bottle hydrogenation device described in Chapter 11 of
Secrets of Methamphetamine Manufacture, Third Edition: .5 gram
platinum in 20 ml distilled water. If this platinum is in the form of
PtO2 instead of reduced platinum metal catalyst obtained with
borohydride, the experimenter must now reduce the platinum by
pressurizing the bottle with hydrogen and stirring fo
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