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or this reaction is about 25° C throughout. When all the methyl nitrite has been bubbled into the reaction mixture, stirring should be continued for another hour. Then, if palladium bromide was used, it should be filtered out. Repeated filtrations will be needed to remove all of the catalyst, because it gets quite finely divided during the course of the reaction. This leaves a clear light-reddish solution. If palladium bromide was used, now adjust pH to 4-7, and allow another hour to complete the hydrolysis. If palladium chloride or the mixed catalyst was used, these substances are soluble in alcohol. In this case, the catalyst will be recovered later. Here, check the pH of the solution again to be sure it is in the proper range before proceeding. Now the alcohol solvent must be removed. This is best done by pouring the reaction mixture into a large filtering flask, stoppering the top of the flask, and removing the solvent under a vacuum. Use of a hot-water bath to speed evaporation is highly recommended for this process. It is not OK to distill off the alcohol at normal pressure, as the heat will cause the nitrite and NO in solution to do bad things to the product. To the residue left in the flask after removal of the alcohol, add some toluene to rinse the product out of the flask into a sep funnel. Next, put 300 ml of water into the flask to dissolve the catalyst if PdCla or the mixed catalyst was used. Add the water solution to the sep funnel to dissolve carried-over catalyst there, then drain this water 12 Studies On The Production OfTMA-2 83 solution of catalyst into a dark bottle and store in the dark until the next batch. If PdBr2 was used, this step can be skipped. Just store the filtered-out PdBra under water in the dark. Now the toluene-phenylacetone solution should be distilled through a Claisen adapter packed with some pieces of broken glass to effect fractionation. The first of the toluene should be distilled at normal pressure to remove water from solution azeotropically. The b.p. of the azeotrope is 85° C, while water-free toluene boils at 110° C. When the water is removed from solution, turn off the heat on the distillation, and carefully apply a vacuum to remove the remainder of the toluene. Then with the vacuum still on, resume heating the flask, and collect the substituted phenylacetone. Methylenedioxyphenylacetone distills at about 140° C and 160° C using a good aspirator with cold water. A poor vacuum source leads to much higher distillation temps and tar formation in the distilling flask. The yield from the reaction is close to 150 ml of phenylacetone. Its color should be clear to a light yellow. The odor of methylenedioxyphenylacetone is much like regular phenylacetone, with a trace of the candy shop odor of the safrole from which it was made. A higher-boiling phenylacetone like 2,4,5-trimethyloxyphenylacetone is better purified as the bisulfite addition product, unless a vacuu Bali Lily Color Blend (Nyphaea sp) Kokain Vaults pdf pdf eaching. Often there are reports of blue glows and jaguars, a holy animal in many endogenous South American cultures. I have been told that McKenna reports that eskimos given an ayahuasca type potion reported seeing large cats, which, of course, are not arctic animals. I however, have found (from admittedly little reading) McKenna's work to be questionable and less than scientific. However, his reports often do parallel others. MAOIs are a class of drugs that all do the same thing: prevent the destruction of monoamines (like DMT). One MAOI is harmaline. Harmaline is easily obtained. Syrian rue is an excellent source. Three grams of seed, extracted with the DMT or eaten alone should suffice. Harmaline containing plants can also be smoked for a more rapid onset. Doses over three grams do not add more potency. Caution should be used with MAOIs. Large doses are hallucinogenic in and of themselves. Large doses are unpleasant and sometimes fatal. The remainder of this section is information cited directly file:///C|/Documents%20and%20Settings/All%20Users/...0Culture/Ayahuasca%20and%20DMT/DMT%20FAQ%202.0.txt (3 of 13)4/14/2004 9:11:34 PM file:///C|/Documents%20and%20Settings/All%20Users/Documents/Bo...%20Counter%20Culture/Ayahuasca%20and%20DMT/DMT%20FAQ%202.0.txt from "Legal Highs" by Twentieth Century Alchemists. They just did a better job than I could do. I have seen this posted around the net and is highly recommended. This information pertains to precautions for MAO inhibitors. READ THEM, KNOW THEM ! You will notice several discrepancies: Legal Highs says that MAOI and mescaline combinations are very dangerous, which contradicts Ott's later reports on the subject. Legal Highs suggests that 5- Me-DMT is a MAOI, which I cannot substantiate. This would render P. tuberosa psychoactive alone. I cannot substantiate this either. > !!DANGEROUS COMBINATIONS!! READ THIS!! VERY IMPORTANT. IGNORING THIS COULD LEAD TO SERIOUS MEDICAL PROBLEMS (like death...) Unless one is very experienced in pharmacology it is unwise to experiment with combinations of drugs. Even when using a single drug, thought should be given to all substances, both food and drug, which have been taken recently. Most primitive people fast or at least abstain from certain substances for several days prior to taking a sacrament. Substances most universally avoided are alcohol, coffee, meat, fat and salt. Some drugs potentiate others. For example, atropine will increase the potency of mescaline, harmine, cannabis and opiates. Many of the substances discussed in this book are MAO inhibitors. MAO (monoamine oxidase) is an enzyme produced in the body which breaks down amines and renders them harmless and ineffective. A MAO inhibitors interfere with the protective enzyme and leaves the body vulnerable to these amines. A common substance such as tyramine, which is usually metabolized with l ayahuasca school Kokain

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