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the empty jug with 100 ml of ether to salvage
any crystals in the jug and pour the ether over the crystals in the filter. After the
ether has passed through the filter repeat the rinsing with another 100 ml of
ether. Then let the crystals dry. If ether is not available or you do not wish to use
such a highly combustible substance, the precipitate and residual benzene can
be poured into a beaker. The jug should be rinsed several more times with a little
benzene and added to the beaker so no crystals are left behind. The beaker is
then placed in a heat bath until all of the benzene has been evaporated.
The next step is to purify the mescaline sulfate crystals. Dissolve the dry crystals
in 200 ml of near-boiling distilled water. Add a pinch of activated charcoal (Norite)
and filter while still hot through number 2 filter paper. The hot water which
contains the mescaline will pass through the filter. The Norite absorbes impurities
from the mescaline. After the liquids have passed through the filter pour a little
more hot water over the filter to rinse through any remaining mescaline which
may have impregnated the filter paper. Add 10 percent ammonia solution a few
drops at a time to the hot filtrates until the solution registers between pH 6.5 and
7. Place a boiling stone in the solution and reduce it's volume to 75 ml by boiling.
Remove the boiling stone and allow the solution to cool to room temperature.
Place the solution in a freezer or in a refrigerator set to the coldest possible
temperature and allow the solution to cool to almost freezing. Tiny white needlelike
crystals form around the bottom and sides of the beaker. Break up the
crystals with a glass stirring rod while the solution is still ice cold and pour
through a filter. Mescaline sulfate is insoluable in near freezing water and will not
pass through the filter. Rinse the beaker with fresh ice water and pour this over
the filter. The crystals will now be pure white and can be dried under a heat lamp
or in an over at 250 degrees F. More mescaline can be salvaged from the water
that has passed through the filter by boiling these liquids down to about 20 ml,
adding Norite while hot, filtering through number 2 paper as before, chilling the
filterate to near freezing as once before, filtering while cold, rinsing with ice water
and drying the crystals. This repetition should obtain at least two more grams of
mescaline sulfate. If large volume mescaline extraction is being conducted it
would be worthwhile to repeat this salvaging procedure several more times.
MIXED ALKALOID EXTRACTIONS
There are numerous methods for extracting a mixture of the alkaloids from cacti.
Different methods may result in varying degrees of purity. For example, the dried,
pulverized material can be defatted with petroleum ether or lighter fluid prior to
extraction to remove lipid content; solvent combinations such as
methanol/chloroform/ammonium hydroxide can be used for extracting; BABY METH TO TO BABY BABY METH How To Recrystalize Meth Avpvresearchchemical
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