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into the benzene during separation pour everything back into the separator, let it
stand and repeat the separation more carefully. It is better to leave some
benzene layer in the water and emulsion than to get emulsion and water into the
benzene. Nothing will be wasted. All of the benzene which contains the
mescaline will eventually be salvaged. Sometimes the layers will fail to separate
properly. If this is the case immerse the funnel or jug in a deep pot of hot water
for two hours. This will break up the emulsion and bring about the separation.
Prepare a solution of 2 parts sulfuric acid and one part water. (never add water to
the acid or it will splatter; add the acid a little at a time to the water by pouring it
down the inside of the graduate or measuring cup containing the water.) Add 25
drops of the acid solution one drop at a time to the benzene extracts. Stopper the
jug and shake well for one minute. Then let stand for five minutes. White streaks
of mescaline sulfates should begin to appear in the benzene. If these do not
appear, shake the jug more vigorously for two to three minutes and let it settle for
five more minutes. I have found that when extracting mescaline from San Pedro
it is sometimes necessary to shake the mixture more thoroughly and for a longer
time to get the mescaline streaks to form. This is probably because of the lower
mescaline content in the plant. This would also apply to any peyote that does not
have a high mescaline content. After the streaks appear add 25 more drops of
the acid solution in the same manner, shake as before and let settle for ten
minutes. More streaks will appear. Add 15 drops of acid, shake and wait 15
minutes for streaks to form. Add 10 drops, shake and wait about 30 minutes.
Test the solution with wide range pH paper. It should show that the solution is
between pH 7.5 and 8. Allow the mescaline sulfate crystals to completely
precipitate. Siphon off as much of the benzene as possible without disturbing the
crystals on the bottom of the jug.
The next steps are to salvage any mescaline still in the water and emulsion layer.
Combine the benzene siphonings with the water/emulsion layer, shake these well
together for 5 minutes and let settle for two hours as before. Carefully remove the
benzene layer, treat it again with acid, precipitate the crystals and siphon off the
benzene as in the previous steps. Recombine the siphoned benzene with the
watery layer and repeat this again and again until no more crystals precipitate.
Siphon off as much benzene as possible without drawing crystals through the
The next step involves removing the remaining benzene from the crystals. There
are two methods to choose from. The first is the quickest, but requires ether,
which is dangerous and often difficult to procure. Shake up the crystals with the
remaining benzene and pour it into a funnel with filter paper. After the benzene
has passed through the filter rinse Mimosa Hostilis Mimosa
Purple/Pink Bark Hawaiian Baby Woodrose
BLUE LILY (NYPHAEA (NYPHAEA crops is
put into a 500 ml flask along with a solution made up of 150 ml ethyl
alcohol, 150 ml water, and 100 grams KOH. Next, 15 ml of hydrazine
hydrate is added.
This hydrazine should be the monohydrate, which is 64% hydrazine. If a weaker variety has been scrounged up, this can be made to work by adding more, and using less water.
Now the flask should be fitted with a condenser, and flushed with nitrogen. Then heat the flask in an oil bath to gentle boiling for 4 hours.
A slow stream of nitrogen to the flask during the reflux averts the danger from hydrazine. The flask is next cooled, and the contents poured into a sep funnel of at least 1000 ml capacity. The batch is then extracted with 600 ml ether, followed by 600 ml of an 85-15% mix of ether and alcohol. Finally, one more extraction with 600 ml of 85-15% ether-alcohol is done. All of the desired product should now be extracted into the solvent, and out of the water. This fact should be checked using a black light to look for the characteristic blue fluorescence. The combined solvent extracts should now be lowered to a pH of about 2 using HC1. At this point, a precipitate should form, and it should be filtered out. The precipitate should be washed free of entrained product with 4-1 ether-alcohol, and the washing added to the rest of the filtered solvent. Now 2750 ml of water should be added to the solvent, and the mixture placed in a gallon and a half glass jug or 5000 ml beaker.
To this should be added 3 portions of cation exchange resin in H* cycle. Cation exchange resin is a common item of commerce used in deionized water systems. Check the yellow pages under "water" and see which of the Ayahuasca Pdf local Culligan men offer deionized water systems. The deionizers come in two-tank systems with one tank packed with cation exchange resin to remove calcium, magnesium and sodium from the water. The other tank has an anion exchange resin to remove chlorides, sulfates, and so on. It is no great task to buy cation exchange resin from these outlets.
The resin consists of tiny plastic beads coated with the exchanger.
In the case of the cation exchangers, Practical LSD Manufacture 44 this is generally a sulfonate.
"In H* cycle" means that the resin is charged up and ready to go. This is generally done by soaking the resin in 20% sulfuric acid in water for a while, then rinsing with distilled water. Check the directions on the container of resin.
Steer clear of mixed resins that contain both anion and cation exchangers. If the Culligan man is too stupid to know the difference, or doesn't know what he has, keep looking until you find one who knows his business. The treatment with three portions of cation exchange resin in H* cycle should be done as follows: Each portion of resin should weigh about 15 grams. The first portion is added, and then the mixture should be stirred strongly or shaken for about 10 minutes. The product will come out of the liquid, and stick Fresh Kratom Extract (Mitragyna speciosa) Hawaiian Baby Woodrose Enhanced Kratom Powder (Mitragyna Speciosa)
nt a bunch of thallium around the house about like you want to be kicked in the teeth with a heavy pair of boots. A further bad aspect of this method is its high cost. 100 grams sell for $150, and the high molecular weight of the compound means that a lot of it has to be used to get a moderate amount of product. One pound of thallium(ni) nitrate is required for a 1-molar batch. This method can be found in Tetrahedron Letters No. 60, pages 5275-80 (1970). To produce a one mole batch, dissolve one mole of propenylbenzene in some methanol, and put it into a one-gallon glass jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate trihydrate in methanol. Then pour the thallium solution into the jug with the propenylbenzene, and stir at room temperature for 5 minutes. The thallium(I) nitrate formed by the reaction comes out of solution. It is removed by filtration. The propenylbenzene has at this point been converted to a ketal. This is hydrolyzed to the phenylacetone by shaking the filtrate with about 2000 ml of 1 molar sulfuric acid solution in water for about 5 minutes. The phenylacetone is then extracted out with a couple of portions of tolulene. This extract is then washed with 5% NaOH solution, then distilled or purified by conversion to the bisulfite addition product. 12 Studies On The Production OfTMA-2 93 Production of TMA-2, MDA, etc. from the Corresponding Phenylacetone There are three good methods for converting the phenylacetone to the psychedelic amphetamine. Choice number one is to use reductive amination with a hydrogenation bomb with Raney nickel, ammonia and alcohol solvent. See Journal of the American Chemical Society, Volume 70, pages 12811-12 (1948). Also see Chem. Abstracts from 1954, column 2097. This gives a yield of about 80% if plenty of Raney nickel is used. The preferred conditions for use with MDA is a temperature of 80 C, and a hydrogen pressure of 50 atmospheres. The drawback to this method is the need for a shaker device for the bomb, and also a heater. The use of platinum as the catalyst in the bomb works great when making MDMA, but gives lousy results when making MDA. There may be a way around this, however, for serious experimenters. It has been found in experiments with phenylacetone that a mixture of ammonia and ammonium chloride produces good yields of amphetamine (50%) when used in a bomb with platinum catalyst. Methylenedioxyphenylacetone is quite likely to behave similarly, along with other phenylacetones. To use this variation, the following materials are placed in the 1.5 liter champagne bottle hydrogenation device described in Chapter 11 of Secrets of Methamphetamine Manufacture, Third Edition: .5 gram platinum in 20 ml distilled water. If this platinum is in the form of PtO2 instead of reduced platinum metal catalyst obtained with borohydride, the experimenter must now reduce the platinum by pressurizing the bottle with hydrogen and stirring fo Ayahuasca Dosage Hawaiian Baby Woodrose Hive Ephedra Fresh Kratom Extract (Mitragyna speciosa) (Some websites, no joke, charge you extra for the funnel Anadenanthera Colubrina Viable Seeds Hawaiian Baby Woodrose Contact