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wnward through the alumina, two zones that fluoresce blue can be spotted by illumination with a black light. The faster-moving zone contains LSD, while the slower-moving zone is iso-LSD. When the zone containing LSD reaches the spigot of the burette, it should be collected in a separate flask. About 3000 ml of the 3-1 benzene-chloroform is required to get the LSD moved down the chromatography column, and finally eluted. The iso-LSD is then flushed from the column by switching the solvent being fed into the top of the column to chloroform. This material is collected in a separate flask, and the solvent removed under a vacuum. The residue is iso-LSD, and should be stored in the freezer until conversion to LSD is undertaken. Directions for this are also given in this chapter. For the fraction containing the LSD, conversion to LSD tartrate must be done to make it water soluble, improve its keeping characteristics, and to allow crystallization. Tartaric acid has the ability to react with two molecules of LSD. Use, then, of a 50% excess of tartaric acid dictates the use of about 1 gram of tartaric acid to 3 grams of LSD. The three grams of LSD would be expected from a well-done batch out of a total 3.5 LSD/iso-LSD mix. The crystalline tartrate is made by dissolving one gram of tartaric acid in a few mis of methanol, and adding this acid solution to the benzene-chloroform elute from the chromatography column. Evaporation of the solvent to a low volume under a vacuum gives crystalline LSD tartrate. Crystals are often difficult to obtain. Instead, an oil may result due to the presence of impurities. This is not cause for alarm; the oil is still likely 90%+ pure. It should be bottled up in dark glass, preferably under a nitrogen atmosphere, and kept in a freezer until moved. If chromatography reveals that one's chosen cooking method produces little of the iso products, then the production of the tartrate salt and crystallization is simplified. The residue obtained at the end Practical LSD Manufacture 32 of the batch is dissolved in a minimum amount of methanol. To this is then added tartaric acid. The same amount is added as above: one gram tartaric acid to three grams LSD. Next, ether is slowly added with vigorous stirring until a precipitate begins to form. The stoppered flask is then put in the freezer overnight to complete the precipitation. After filtering or centrifuging to isolate the product, it is transferred to a dark bottle, preferably under nitrogen, and kept in the freezer until moved. LSD from (so-LSD Two variations on this procedure will be presented here. The first is the method of Smith and Timmis from The Journal of the Chemistry Society Volume 139, H pages 1168-1169 (1936). The other is found in US patent 2,736,728. Both use the action of a strong hydroxide solution to convert iso material into a mixture that contains active and iso material. At equilibrium, the mixture contains about 2/3 Terscheckii Cactus Skin Cuts (Trichocereus Terscheckii) Extrakt Caupuri Caapi Vine (Banisteriopsis caapi) lt-up pressure from the flask. If the stirring bar bangs too violently in the flask, remove it with a magnet rather than break the flask. Pour the contents of the flask into a 250 ml sep funnel, and drain the lower layer (water solution of lysergic acid hydrazide tartarate) into a 250 ml Erlenmeyer flask wrapped in foil. To the ether layer still in the sep funnel, add 50 ml fresh decimolar tartaric-acid solution, and shake. Examine the water layer for the presence of lysergic acid hydrazide with a black light. If there is a significant amount, add this also to the Erlenmeyer flask. Place the magnetic stirring bar in the Erlenmeyer flask, and stir it moderately. Monitor the pH of the solution with a properly calibrated pH meter, and slowly add .5M (20 grams per liter) sodium hydroxide solution until the pH has risen to the range of 8-8.5. Higher pH will cause racemization. The freebase is then extracted from the water solution with chloroform. Two extractions with 100 ml of chloroform should complete the extraction, but check a third extraction with the black light to ensure that most all of the product lysergic acid hydrazide has been extracted. The chloroform extracts should be evaporated under a vacuum in a 500 ml flask to yield the product. This is best done by rigging the 500 ml flask for simple distillation, and applying an aspirator vacuum to remove the chloroform. Assume that the yield from this procedure will be about 5 grams of lysergic acid hydrazide if ergot was the crop used. Assume that the yield will be about 7.5 grams if seeds were used. The difference here is due to the fact that in ergot, the amides 4 LSD Directly From The Lysergic Amides — The One Pot Shot 27 are largely composed of substances in which the portion lopped off is about as large as the lysergic acid molecule. Seeds tend to be more conservative as to their building upon the lysergic molecule. A careful weighing on a sensitive scale comparing the weight of the flask before and after would give a more exact number. Both of these choices are really very poor, because lysergic acid hydrazide, unlike most other lysergic compounds, crystallizes very well with negligible loss of product. At the hydrazide stage of LSD manufacture, one has a perfect opportunity to get an exceedingly pure product, freed from clavine alkaloids and other garbage compounds carried in from the extraction of the complex plant material. I refer the reader to US patent 2,090,429 issued to Albert Hofmann and Arthur Stoll, the dynamic duo of lysergic chemistry, dealing with lysergic acid hydrazide. In this patent, they describe in a rather excited state how they were able to produce pure lysergic acid hydrazide from tank scrapings that were otherwise impure junk. Lysergic acid hydrazide has the following properties: it dissolves easily in acid, but is very difficultly soluble in water, ether, benzene and chloroform. In hot absolute ethanol it is slightly Asian Lotus (Nelumbo nucifera) DRIED FLOWERS Extrakt erowid ayahuasca

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