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put into a 500 ml flask along with a solution made up of 150 ml ethyl
alcohol, 150 ml water, and 100 grams KOH. Next, 15 ml of hydrazine
hydrate is added. This hydrazine should be the monohydrate, which is
If a weaker variety has been scrounged up, this can be
made to work by adding more, and using less water.
Now the flask should be fitted with a condenser, and flushed with
nitrogen. Then heat the flask in an oil bath to gentle boiling for 4
hours. A slow stream of nitrogen to the flask during the reflux averts
the danger from hydrazine.
The flask is next cooled, and the contents poured into a sep funnel of
at least 1000 ml capacity.
The batch is then extracted with 600 ml
ether, followed by 600 ml of an 85-15% mix of ether and alcohol.
Finally, one more extraction with 600 ml of 85-15% ether-alcohol is
All of the desired product should now be extracted into the
solvent, and out of the water. This fact should be checked using a
black light to look for the characteristic blue fluorescence.
The combined solvent extracts should now be lowered to a pH of
about 2 using HC1. At this point, a precipitate should form, and it
should be filtered out. The precipitate should be washed free of
entrained product with 4-1 ether-alcohol, and the washing added to
the rest of the filtered solvent.
Now 2750 ml of water should be added to the solvent, and the
mixture placed in a gallon and a half glass jug or 5000 ml beaker. To
this should be added 3 portions of cation exchange resin in H* cycle.
Cation exchange resin is a common item of commerce used in
deionized water systems.
Check the yellow pages under "water" and
see which of the local Culligan men offer deionized water systems.
The deionizers come in two-tank systems with one tank packed with
cation exchange resin to remove calcium, magnesium and sodium
from the water. The other tank has an anion exchange resin to remove
chlorides, sulfates, and so on. It is no great task to buy cation
exchange resin from these outlets. The resin consists of tiny plastic
beads coated with the exchanger.
In the case of the cation exchangers,
Practical LSD Manufacture
this is generally a sulfonate.
"In H* cycle" means that the resin is
charged up and ready to go. This is generally done by soaking the
resin in 20% sulfuric acid in water for a while, then rinsing with
distilled water. Check the directions on the container of resin. Steer
clear of mixed resins that contain both anion and cation exchangers. If
the Culligan man is too stupid to know the difference, or doesn't
know what he has, keep looking until you find one who knows his
The treatment with three portions of cation exchange resin in H*
cycle should be done as follows: Each portion of resin should weigh
about 15 grams. The first portion is added, and then the mixture
should be stirred strongly or shaken for about 10 minutes. The product
will come out of the liquid, and stick
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Android-App://Com.Google.Android.Googlequicksearchbox/Https/Www.Google.Com ing in the cold before then adding 25 ml of diethylamine.
Stir for an additional 10 minutes, then pour the batch into a 2000
ml sep funnel. Now to the sep funnel add 800 ml of water. Mix this in
thoroughly, then add 400 ml of saturated salt solution in water. Mix
this in, then extract out the LSD by repeated extraction with 250 ml
portions of ethylene dichloride. Check with a blacklight for complete
6 LSD From Lysergic Acid And SO3
The combined ethylene dichloride extracts should be evaporated
under a vacuum as above, and the residue of LSD and iso-LSD should be
separated and treated as above.
LSD From Lysergic Acid And
LSD From Lysergic Acid
And Trifluoroacetic Anhydride
This method is a little bit lame, but it may be the method of choice if
trifluoroacetic anhydride or trifluoroacetic acid should happen to fall
from the sky into one's hands. The reason why this method is a bit lame
is threefold. Anhydrous lysergic acid is required for this reaction. To
obtain anhydrous lysergic acid, the lysergic acid hydrate yielded by the
methods in Chapter 5 must be baked under high vacuum for a
couple hours. This is obviously not good for such a delicate molecule.
The water molecule will be shed by a baking temperature of 120° C at a
vacuum of 1 mm Hg, 140° C at 2 mm Hg, and still higher
temperatures at less perfect vacuums. A MacLeod gauge is the only
instrument that I know of which is capable of accurately measuring
such high vacuums.
Another reason why this method is lacking is that the yields are
not so good as those achieved by the other synthetic routes presented in
this book. It is possible to recover the unreacted lysergic acid at the end
of the process, but this does not make up for the initial lower yield,
not to mention the added hassle of recovering and redrying the lysergic
Strike number three for this route is its propensity to give byproducts
that are difficult to separate from the desired product. I am
Practical LSD Manufacture
not talking here about the large amount of iso-LSD that this method
makes. That molecular jumbling is inconsequential, because the
lysergic acid used is itself an isomeric mixture. Rather, what can
occur here is the production of LSD and other by-products.
The mechanics of this reaction are similar to the reaction with
SOs, in that two molecules of the anhydride react with the lysergic
acid molecule to form the mixed anhydride. In this reaction, there is
no need to first react the lysergic acid with hydroxide to form the
metal salt. Also, the need to follow exact stoichiometric quantities of
reactants is not as pressing as in the SO$ method.
To do the reaction, into a 1000 ml flask (carefully dried and
equipped with a magnetic stirring bar) place 16 grams of lysergic acid
and 375 ml of acetonitrile. The lysergic acid will not dissolve. Stopper
the flask and place it in the freezer to cool the contents to -20f
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ayahausca nt a bunch of
thallium around the house about like you want to be kicked in the
teeth with a heavy pair of boots.
A further bad aspect of this method is its high cost. 100 grams sell
for $150, and the high molecular weight of the compound means that a
lot of it has to be used to get a moderate amount of product. One
pound of thallium(ni) nitrate is required for a 1-molar batch.
This method can be found in Tetrahedron Letters No. 60, pages
5275-80 (1970). To produce a one mole batch, dissolve one mole of
propenylbenzene in some methanol, and put it into a one-gallon glass
jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate
trihydrate in methanol. Then pour the thallium solution into the jug
with the propenylbenzene, and stir at room temperature for 5 minutes.
The thallium(I) nitrate formed by the reaction comes out of solution. It is
removed by filtration.
The propenylbenzene has at this point been converted to a ketal.
This is hydrolyzed to the phenylacetone by shaking the filtrate with
about 2000 ml of 1 molar sulfuric acid solution in water for about 5
minutes. The phenylacetone is then extracted out with a couple of
portions of tolulene. This extract is then washed with 5% NaOH
solution, then distilled or purified by conversion to the bisulfite
12 Studies On The Production OfTMA-2
Production of TMA-2, MDA, etc. from the
There are three good methods for converting the phenylacetone to
the psychedelic amphetamine. Choice number one is to use reductive
amination with a hydrogenation bomb with Raney nickel, ammonia
and alcohol solvent. See Journal of the American Chemical Society,
Volume 70, pages 12811-12 (1948). Also see Chem. Abstracts from
1954, column 2097. This gives a yield of about 80% if plenty of
Raney nickel is used. The preferred conditions for use with MDA is a
temperature of 80 C, and a hydrogen pressure of 50 atmospheres.
The drawback to this method is the need for a shaker device for
the bomb, and also a heater. The use of platinum as the catalyst in the
bomb works great when making MDMA, but gives lousy results when
making MDA. There may be a way around this, however, for serious
experimenters. It has been found in experiments with phenylacetone
that a mixture of ammonia and ammonium chloride produces good
yields of amphetamine (50%) when used in a bomb with platinum
catalyst. Methylenedioxyphenylacetone is quite likely to behave
similarly, along with other phenylacetones.
To use this variation, the following materials are placed in the 1.5
liter champagne bottle hydrogenation device described in Chapter 11 of
Secrets of Methamphetamine Manufacture, Third Edition: .5 gram
platinum in 20 ml distilled water. If this platinum is in the form of
PtO2 instead of reduced platinum metal catalyst obtained with
borohydride, the experimenter must now reduce the platinum by
pressurizing the bottle with hydrogen and stirring fo
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@Tuesday, January 22, 2019 2:08:04 PM