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nt a bunch of thallium around the house about like you want to be kicked in the teeth with a heavy pair of boots.
A further bad aspect of this method is its high cost. 100 grams sell for $150, and the high molecular weight of the compound means that a lot of it has to be used to get a moderate amount of product. One pound of thallium(ni) nitrate is required for a 1-molar batch. This method can be found in Tetrahedron Letters No. 60, pages 5275-80 (1970). To produce a one mole batch, dissolve one mole of propenylbenzene in some methanol, and put it into a one-gallon glass jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate trihydrate in methanol.
Then pour the thallium solution into the jug with the propenylbenzene, and stir at room temperature for 5 minutes.
The thallium(I) nitrate formed by the reaction comes out of solution. It is removed by filtration.
The propenylbenzene has at this point been converted to a ketal.
This is hydrolyzed to the phenylacetone by shaking the filtrate with about 2000 ml of 1 molar sulfuric acid solution in water for about 5 minutes. The phenylacetone is then extracted out with a couple of portions of tolulene. This extract is then washed with 5% NaOH solution, then distilled or purified by conversion to the bisulfite addition product. 12 Studies On The Production OfTMA-2 93 Production of TMA-2, MDA, etc. from the Corresponding Phenylacetone There are three good methods for converting the phenylacetone to the psychedelic amphetamine. Choice number one is to use reductive amination

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with a hydrogenation bomb with Raney nickel, ammonia and alcohol solvent. See Journal of the American Chemical Society, Volume 70, pages 12811-12 (1948).
Also see Chem. Abstracts from 1954, column 2097. This gives a yield of about 80% if plenty of Raney nickel is used. The preferred conditions for use with MDA is a temperature of 80 C, and a hydrogen pressure of 50 atmospheres.
The drawback to this method is the need for a shaker device for the bomb, and also a heater.
The use of platinum as the catalyst in the bomb works great when making MDMA, but gives lousy results

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when making MDA. There may be a way around this, however, for serious experimenters. It has been found in experiments with phenylacetone that a mixture of ammonia and ammonium chloride produces good yields of amphetamine (50%) when used in a bomb with platinum catalyst.
Methylenedioxyphenylacetone is quite likely to behave similarly, along with other phenylacetones. To use this variation, the following materials are placed in the 1.
5 liter champagne bottle hydrogenation device described in Chapter 11 of Secrets of Methamphetamine Manufacture, Third Edition: .5 gram platinum in 20 ml distilled water. If this platinum is in the form of PtO2 instead of reduced platinum metal catalyst obtained with borohydride, the experimenter must now reduce the platinum by pressurizing the bottle with hydrogen and stirring fo

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