the alumina, two zones that fluoresce blue can be spotted by
illumination with a black light. The faster-moving zone contains LSD,
while the slower-moving zone is iso-LSD.
When the zone containing LSD reaches the spigot of the burette, it
should be collected in a separate flask. About 3000 ml of the 3-1
benzene-chloroform is required to get the LSD moved down the
chromatography column, and finally eluted.
The iso-LSD is then flushed from the column by switching the
solvent being fed into the top of the column to chloroform. This
material is collected in a separate flask, and the solvent removed
under a vacuum. The residue is iso-LSD, and should be stored in the
freezer until conversion to LSD is undertaken. Directions for this are
also given in this chapter.
For the fraction containing the LSD, conversion to LSD tartrate
must be done to make it water soluble, improve its keeping
characteristics, and to allow crystallization. Tartaric acid has the
ability to react with two molecules of LSD. Use, then, of a 50% excess of
tartaric acid dictates the use of about 1 gram of tartaric acid to 3
grams of LSD. The three grams of LSD would be expected from a
well-done batch out of a total 3.5 LSD/iso-LSD mix.
The crystalline tartrate is made by dissolving one gram of tartaric
acid in a few mis of methanol, and adding this acid solution to the
benzene-chloroform elute from the chromatography column.
Evaporation of the solvent to a low volume under a vacuum gives
crystalline LSD tartrate. Crystals are often difficult to obtain. Instead,
an oil may result due to the presence of impurities. This is not cause
for alarm; the oil is still likely 90%+ pure. It should be bottled up in
dark glass, preferably under a nitrogen atmosphere, and kept in a
freezer until moved.
If chromatography reveals that one's chosen cooking method
produces little of the iso products, then the production of the tartrate
salt and crystallization is simplified. The residue obtained at the end
Practical LSD Manufacture
of the batch is dissolved in a minimum amount of methanol. To this is
then added tartaric acid. The same amount is added as above: one gram
tartaric acid to three grams LSD. Next, ether is slowly added with
vigorous stirring until a precipitate begins to form. The stoppered flask is
then put in the freezer overnight to complete the precipitation. After
filtering or centrifuging to isolate the product, it is transferred to a dark
bottle, preferably under nitrogen, and kept in the freezer until moved.
LSD from (so-LSD
Two variations on this procedure will be presented here. The first is
the method of Smith and Timmis from The Journal of the
Chemistry Society Volume 139, H pages 1168-1169 (1936). The other is
found in US patent 2,736,728. Both use the action of a strong
hydroxide solution to convert iso material into a mixture that contains
active and iso material. At equilibrium, the mixture contains about 2/3
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bufotenine for sale e mental discipline. People who cannot endure the
bitterness of peyote often go to various extremes to get it into the system without
having to taste it. One fairly effective method is to drink unsweetened grapefruit
juice while chewing it. The acids in the juice somewhat neutralize some of the
bitter bases. Another method is to grind the dried buttons in a pepper grinder and
pack the pulverised material into OOO capsules which are washed down with
warm water. This is an effective method but it can take 20 capsules or more to
get a 350mg dose of mescaline. Often people will boil the buttons in water for
several hours to make a concentrated tea. A cup of this decoction can be
swallowed in a few hasty gulps. Another preparation that is occasionally used is
a jello-type dessert made with the fresh or dried plant. If spoonfulls are
swallowed whole the gelatine serves as a sort of shield protecting the tastebuds
from contact with the bitter material. It also slows down the the absorption of the
drug in the digestive tract. This can be of value. It is generally recommended that
anyone consuming peyote or mescaline ingest it gradually during a period of an
hour or take two half doses 45 minutes apart. This is done to reduce the shock of
the alkaloid to the system. Nausea or queasiness is sometimes experienced half
an hour or so after taking peyote or mescaline. This usually passes in less than
an hour. A sip of grapefruit juice will sometimes dispel the sick feeling. During the
peyote ceremony Indians encourage vomiting rather than restraint if the urge
presents itself. Throwing up, they believe, is apurging of both physical and
spiritual ills. Most tribes fast for at least a day before taking peyote. This can also
help to minimize gastric distress. One should not have eaten for at least 6 hours
before taking either mescaline or peyote.
A method which avoids both the bitterness and the nausea is the rectal infusion.
8-16 grams of dried peyote is ground into a fine powder and boiled in a pint of
water for 30 minutes. It is then strained and further boiled to reduce it's volume to
one half pint. After cooling, this is taken as an enema using a small bulb syringe
and retained for at least two hours. If there is any fecal matter in the lower bowel,
a small cleansing enema should be taken and thoroughly expelled before having
the peyote infusion. Otherwise much of the drug will be taken up by the feces
and later voided.
FINDING AND PICKING PEYOTE
The peyote cactus may be found in many areas throughout the Chihuahuan
Desert from central Mexico to southern Texas. When a site is found where
peyote grows it usually does so in abundance. Sometimes it grows in open sunlit
places, but more often it is found in clusters under fairly large shrubs, among
mesquite or creosote bushes or in the shade of large succulents.
The best time to harvest any cactus is after a long dry spell. The worst time is
during or after a rainy period.
Purple/Pink Mimosa Hostilis Root Bark Ayahuascavine PREPARATION PREPARATION
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