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o get into the benzene during separation pour everything back into the separator, let it stand and repeat the separation more carefully. It is better to leave some benzene layer in the water and emulsion than to get emulsion and water into the benzene. Nothing will be wasted. All of the benzene which contains the mescaline will eventually be salvaged. Sometimes the layers will fail to separate properly. If this is the case immerse the funnel or jug in a deep pot of hot water for two hours. This will break up the emulsion and bring about the separation. Prepare a solution of 2 parts sulfuric acid and one part water. (never add water to the acid or it will splatter; add the acid a little at a time to the water by pouring it down the inside of the graduate or measuring cup containing the water.) Add 25 drops of the acid solution one drop at a time to the benzene extracts. Stopper the jug and shake well for one minute. Then let stand for five minutes. White streaks of mescaline sulfates should begin to appear in the benzene. If these do not appear, shake the jug more vigorously for two to three minutes and let it settle for five more minutes. I have found that when extracting mescaline from San Pedro it is sometimes necessary to shake the mixture more thoroughly and for a longer time to get the mescaline streaks to form. This is probably because of the lower mescaline content in the plant. This would also apply to any peyote that does not have a high mescaline content. After the streaks appear add 25 more drops of the acid solution in the same manner, shake as before and let settle for ten minutes. More streaks will appear. Add 15 drops of acid, shake and wait 15 minutes for streaks to form. Add 10 drops, shake and wait about 30 minutes. Test the solution with wide range pH paper. It should show that the solution is between pH 7.5 and 8. Allow the mescaline sulfate crystals to completely precipitate. Siphon off as much of the benzene as possible without disturbing the crystals on the bottom of the jug. The next steps are to salvage any mescaline still in the water and emulsion layer. Combine the benzene siphonings with the water/emulsion layer, shake these well together for 5 minutes and let settle for two hours as before. Carefully remove the benzene layer, treat it again with acid, precipitate the crystals and siphon off the benzene as in the previous steps. Recombine the siphoned benzene with the watery layer and repeat this again and again until no more crystals precipitate. Siphon off as much benzene as possible without drawing crystals through the siphon. The next step involves removing the remaining benzene from the crystals. There are two methods to choose from. The first is the quickest, but requires ether, which is dangerous and often difficult to procure. Shake up the crystals with the remaining benzene and pour it into a funnel with filter paper. After the benzene has passed through the filter rinse android-app://com.google.android.googlequicksearchbox/ Ayahuasca Preparation San Pedro Cactus (Trichocereus pachanoi)De-cored Dried Outer Skin wnward through the alumina, two zones that fluoresce blue can be spotted by illumination with a black light. The faster-moving zone contains LSD, while the slower-moving zone is iso-LSD. When the zone containing LSD reaches the spigot of the burette, it should be collected in a separate flask. About 3000 ml of the 3-1 benzene-chloroform is required to get the LSD moved down the chromatography column, and finally eluted. The iso-LSD is then flushed from the column by switching the solvent being fed into the top of the column to chloroform. This material is collected in a separate flask, and the solvent removed under a vacuum. The residue is iso-LSD, and should be stored in the freezer until conversion to LSD is undertaken. Directions for this are also given in this chapter. For the fraction containing the LSD, conversion to LSD tartrate must be done to make it water soluble, improve its keeping characteristics, and to allow crystallization. Tartaric acid has the ability to react with two molecules of LSD. Use, then, of a 50% excess of tartaric acid dictates the use of about 1 gram of tartaric acid to 3 grams of LSD. The three grams of LSD would be expected from a well-done batch out of a total 3.5 LSD/iso-LSD mix. The crystalline tartrate is made by dissolving one gram of tartaric acid in a few mis of methanol, and adding this acid solution to the benzene-chloroform elute from the chromatography column. Evaporation of the solvent to a low volume under a vacuum gives crystalline LSD tartrate. Crystals are often difficult to obtain. Instead, an oil may result due to the presence of impurities. This is not cause for alarm; the oil is still likely 90%+ pure. It should be bottled up in dark glass, preferably under a nitrogen atmosphere, and kept in a freezer until moved. If chromatography reveals that one's chosen cooking method produces little of the iso products, then the production of the tartrate salt and crystallization is simplified. The residue obtained at the end Practical LSD Manufacture 32 of the batch is dissolved in a minimum amount of methanol. To this is then added tartaric acid. The same amount is added as above: one gram tartaric acid to three grams LSD. Next, ether is slowly added with vigorous stirring until a precipitate begins to form. The stoppered flask is then put in the freezer overnight to complete the precipitation. After filtering or centrifuging to isolate the product, it is transferred to a dark bottle, preferably under nitrogen, and kept in the freezer until moved. LSD from (so-LSD Two variations on this procedure will be presented here. The first is the method of Smith and Timmis from The Journal of the Chemistry Society Volume 139, H pages 1168-1169 (1936). The other is found in US patent 2,736,728. Both use the action of a strong hydroxide solution to convert iso material into a mixture that contains active and iso material. At equilibrium, the mixture contains about 2/3 ayahuasca kit Ayahuasca Preparation Caupuri Caapi Vine (Banisteriopsis caapi)

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99 In Stock Party Pack (3 Items) Click to view product details Party Pack (3 Items) RRP: $168 Viable Colubrina Viable Anadenanthera Anadenanthera Ayahuasca Preparation Cactus Cuzco Cactus Vendor Trichocereus Dmt 4 Dmt Cuzco ing in the cold before then adding 25 ml of diethylamine. Stir for an additional 10 minutes, then pour the batch into a 2000 ml sep funnel. Now to the sep funnel add 800 ml of water. Mix this in thoroughly, then add 400 ml of saturated salt solution in water. Mix this in, then extract out the LSD by repeated extraction with 250 ml portions of ethylene dichloride. Check with a blacklight for complete extraction. 6 LSD From Lysergic Acid And SO3 55 The combined ethylene dichloride extracts should be evaporated under a vacuum as above, and the residue of LSD and iso-LSD should be separated and treated as above. 7 LSD From Lysergic Acid And Trifluoroacetic Anhydride 51 1 LSD From Lysergic Acid And Trifluoroacetic Anhydride This method is a little bit lame, but it may be the method of choice if trifluoroacetic anhydride or trifluoroacetic acid should happen to fall from the sky into one's hands. The reason why this method is a bit lame is threefold. Anhydrous lysergic acid is required for this reaction. To obtain anhydrous lysergic acid, the lysergic acid hydrate yielded by the methods in Chapter 5 must be baked under high vacuum for a couple hours. This is obviously not good for such a delicate molecule. The water molecule will be shed by a baking temperature of 120° C at a vacuum of 1 mm Hg, 140° C at 2 mm Hg, and still higher temperatures at less perfect vacuums. A MacLeod gauge is the only instrument that I know of which is capable of accurately measuring such high vacuums. Another reason why this method is lacking is that the yields are not so good as those achieved by the other synthetic routes presented in this book. It is possible to recover the unreacted lysergic acid at the end of the process, but this does not make up for the initial lower yield, not to mention the added hassle of recovering and redrying the lysergic acid. Strike number three for this route is its propensity to give byproducts that are difficult to separate from the desired product. I am Practical LSD Manufacture 58 not talking here about the large amount of iso-LSD that this method makes. That molecular jumbling is inconsequential, because the lysergic acid used is itself an isomeric mixture. Rather, what can occur here is the production of LSD and other by-products. The mechanics of this reaction are similar to the reaction with SOs, in that two molecules of the anhydride react with the lysergic acid molecule to form the mixed anhydride. In this reaction, there is no need to first react the lysergic acid with hydroxide to form the metal salt. Also, the need to follow exact stoichiometric quantities of reactants is not as pressing as in the SO$ method. To do the reaction, into a 1000 ml flask (carefully dried and equipped with a magnetic stirring bar) place 16 grams of lysergic acid and 375 ml of acetonitrile. The lysergic acid will not dissolve. Stopper the flask and place it in the freezer to cool the contents to -20f Ayawaska Ayahuasca Preparation ayahuascasearch

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