Ayahuasca RED Vine (Banisteriopsis caapi)
“CHALIPONGA” Dried Whole Leaf (Diplopterys cabrerana)
put into a 500 ml flask along with a solution made up of 150 ml ethyl
alcohol, 150 ml water, and 100 grams KOH. Next, 15 ml of hydrazine
hydrate is added. This hydrazine should be the monohydrate, which is
64% hydrazine. If a weaker variety has been scrounged up, this can be
made to work by adding more, and using less water.
Now the flask should be fitted with a condenser, and flushed with
nitrogen. Then heat the flask in an oil bath to gentle boiling for 4
hours. A slow stream of nitrogen to the flask during the reflux averts
the danger from hydrazine.
The flask is next cooled, and the contents poured into a sep funnel of
at least 1000 ml capacity. The batch is then extracted with 600 ml
ether, followed by 600 ml of an 85-15% mix of ether and alcohol.
Finally, one more extraction with 600 ml of 85-15% ether-alcohol is
All of the desired product should now be extracted into the
solvent, and out of the water. This fact should be checked using a
black light to look for the characteristic blue fluorescence.
The combined solvent extracts should now be lowered to a pH of
about 2 using HC1. At this point, a precipitate should form, and it
should be filtered out. The precipitate should be washed free of
entrained product with 4-1 ether-alcohol, and the washing added to
the rest of the filtered solvent.
Now 2750 ml of water should be added to the solvent, and the
mixture placed in a gallon and a half glass jug or 5000 ml beaker. To
this should be added 3 portions of cation exchange resin in H* cycle.
Cation exchange resin is a common item of commerce used in
deionized water systems. Check the yellow pages under "water" and
see which of the local Culligan men offer deionized water systems.
The deionizers come in two-tank systems with one tank packed with
cation exchange resin to remove calcium, magnesium and sodium
from the water. The other tank has an anion exchange resin to remove
chlorides, sulfates, and so on. It is no great task to buy cation
exchange resin from these outlets. The resin consists of tiny plastic
beads coated with the exchanger. In the case of the cation exchangers,
Practical LSD Manufacture
this is generally a sulfonate. "In H* cycle" means that the resin is
charged up and ready to go. This is generally done by soaking the
resin in 20% sulfuric acid in water for a while, then rinsing with
distilled water. Check the directions on the container of resin. Steer
clear of mixed resins that contain both anion and cation exchangers. If
the Culligan man is too stupid to know the difference, or doesn't
know what he has, keep looking until you find one who knows his
The treatment with three portions of cation exchange resin in H*
cycle should be done as follows: Each portion of resin should weigh
about 15 grams. The first portion is added, and then the mixture
should be stirred strongly or shaken for about 10 minutes. The product
will come out of the liquid, and stick CAAPI) RED RED (BANISTERIOPSIS VINE Ayahuasca Preparation
ayahuasca recipe Damiana Bliss Drops 37g $14 Ayahuasca Preparation
alse Peyote. These people make long pilgrimages to the
sacred places where peyote grows in search of that sacrement. They believe that
if a person is has not been properly purified the spirits will lead him to the False
Peyote and if he partakes of it, he will suffer madness or at least a bad trip. The
plant is known among some tribes as Chautle or Chaute.
These names are also
used for other Ariocarpus species. This cactus contains hordenine, Nmethyltryamine
in fairly small amounts (about
“CHALIPONGA” Dried Whole Leaf (Diplopterys cabrerana) 0.02 percent) and traces of Nmethyl-
3,4-dimethoxy-B-phenethylamine, and N-methyl-4-B-phenethylamine.
Aside from these alkaloids it also contains a flavone called retusin (3,3',4',7-
tetramethoxy-5-hydroxyflavone). Although alkaloid content may very some at
different seasons or stages of growth, from the scientific point of view the
amounts present in this plant appear insufficient to produce any
SUNAMI: This plant, ARIOCARPUS FISSURATUS, has been used in folkoric
medicine of Mexico and southwestern USA. It is believed to be more potent than
peyote and is used in the same manner as that cactus or made into an
intoxicating drink. sp) Color
Bali Lily Color sp) sp) Among some tribes it is known as Chaute (a generic term for
Ariocarpus species), living rock, or dry whiskey.
The sp) Color
Bali Lily Color sp) sp) latter name, however, is
often used for peyote and other psychoactive cacti. There are two varieties of A.
fissuratus: var. lloydii and var. fissuratus. Both have about the same
The plant contains mostly hordenine, less N-methyltyramine
and some N-methyl-3,4-dimethoxy-B-phenethylamine. Two other
species, A. kotschoubeyanus also known as Pata De Venado or Pezuna De
Venado, and A. trigonus also contain these alkaloids.
DOÑANA: This small cactus, CORYPHANTHA MACROMERIS, from northern
Mexico has been found to contain macromerine, a phenethylamine drug reputed
to have about 1/5 the potency of mescaline. It also contains normacromerine, Nformylnor-
macromerin, tyramine, N-methyltramine, hordenine, N-methyl-3,4-
dimethoxy-B-phenethylamine, metanephrine, and synephrine (a macromerine
Other coryphantha species which contain macromerine with most of
these other alkaloids include: C. pectinada, C. elephantideus, C. runyonii and C.
cornifera var. echinus.
Most of these alkaloids with the exception of macromerine
have also been found in other varieties of C. conifera and in C. durangensis, C.
ottonis, C. poselgeriana and C. ramillosa. Considering that there is usually no
more than 0.1 percent macromerine in Doñana and that a gram or more of this
alkaloid may be needed to produce a psychotropic effect, one would have to
consume more than a kilo of the dried cactus or 20 pounds of the fresh plant.
Ayahuasca YELLOW Vine (Banisteriopsis caapi)
this is not possible for most humans. If one wishes to experiment with the
hallucinogenic properties of Doñana, is is necessary first to make an extraction of
the mixed alkaloids. Methods for this are given latter in this guide.
DOLICH Ayahuasca Preparation Recreational
“Chaliponga” Dried Whole Leaf (Diplopterys Cabrerana) or this reaction is about 25° C throughout.
When all the methyl nitrite has been bubbled into the reaction
mixture, stirring should be continued for another hour. Then, if
palladium bromide was used, it should be filtered out. Repeated
filtrations will be needed to remove all of the catalyst, because it gets
quite finely divided during the course of the reaction. This leaves a
clear light-reddish solution. If palladium bromide was used, now
adjust pH to 4-7, and allow another hour to complete the hydrolysis.
If palladium chloride or the mixed catalyst was used, these
substances are soluble in alcohol. In this case, the catalyst will be
recovered later. Here, check the pH of the solution again to be sure it is
in the proper range before proceeding.
Now the alcohol solvent must be removed. This is best done by
pouring the reaction mixture into a large filtering flask, stoppering the
top of the flask, and removing the solvent under a vacuum. Use of a
hot-water bath to speed evaporation is highly recommended for this
process. It is not OK to distill off the alcohol at normal pressure, as
the heat will cause the nitrite and NO in solution to do bad things to the
To the residue left in the flask after removal of the alcohol, add
some toluene to rinse the product out of the flask into a sep funnel.
Next, put 300 ml of water into the flask to dissolve the catalyst if
PdCla or the mixed catalyst was used. Add the water solution to the
sep funnel to dissolve carried-over catalyst there, then drain this water
12 Studies On The Production OfTMA-2
solution of catalyst into a dark bottle and store in the dark until the
next batch. If PdBr2 was used, this step can be skipped. Just store the
filtered-out PdBra under water in the dark.
Now the toluene-phenylacetone solution should be distilled
through a Claisen adapter packed with some pieces of broken glass to
effect fractionation. The first of the toluene should be distilled at
normal pressure to remove water from solution azeotropically. The
b.p. of the azeotrope is 85° C, while water-free toluene boils at 110° C.
When the water is removed from solution, turn off the heat on the
distillation, and carefully apply a vacuum to remove the remainder of
the toluene. Then with the vacuum still on, resume heating the flask,
and collect the substituted phenylacetone. Methylenedioxyphenylacetone
distills at about 140° C and 160° C using a good aspirator
with cold water. A poor vacuum source leads to much higher
distillation temps and tar formation in the distilling flask. The yield
from the reaction is close to 150 ml of phenylacetone. Its color should be
clear to a light yellow. The odor of methylenedioxyphenylacetone is
much like regular phenylacetone, with a trace of the candy shop odor
of the safrole from which it was made.
A higher-boiling phenylacetone like 2,4,5-trimethyloxyphenylacetone
is better purified as the bisulfite addition product, unless a
ayahuasca school Ayahuasca Preparation
San Pedro Cactus (Trichocereus pachanoi)De-cored Dried Outer Skin
@Tuesday, September 25, 2018 5:10:18 PM