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extractions can be made acidic (pH 9.5) with 1-N hydrochloric acid, filtered and
washed in a separatory funnel or improvised siphon-jug apparatus with diethyl
ether, neutralized with ammonium hydroxide and evaporated to dryness.
However, most of these solvents are difficult for the non-professional to obtain.
Perhaps it is just as well since many of these solvents are either toxic or
explosive if handled improperly. Also, we do not always know precisely what we
are trying to extract. Some of the active principles may be non-alkaloidal. Too
much purification might remove some of the active substances. The approach
given here employs materials which may be purchased inexpensively at any
supermarket and are safe to work with. This procedure extracts all of the alcohol
and water-soluable alkaloids and non-alkaloidal materials and permits only the
fibrous pulp to be discarded.
Pulverize the dried cactus (tufts and spines need not be removed). Prepare a
mixture of two parts isopropyl rubbing alcohol and one part clear, non-sudsing,
unscented and untinted ammonia. Make the pulverized material soggy with this
mixture and allow it to stand covered overnight. Do not use aluminum or iron
wares during any of these steps. After soaking, cover the mash with isopropyl
alcohol and boil in a heat bath for six hours. Strain the liquids through muslin and
press as much liquid as possible from the pulp. With fresh alcohol repeat the
boiling and straining three more times. Combine the strained liquids. Evaporate
this in a heat bath until only a tar remains. (When evaporating a solvent use and
electric range or hot plate rather than a gas stove. Have adequate ventilation and
avoid breathing the fumes.) The tar can be further dried by spreading it thinly on
a baking tray and placing it in an oven set at the lowest possible heat. Remove
the tray once every fifteen minutes to examine the material. When it appears to
be almost dry place it back in the oven, shut the heat off, and let it stay there until
the oven cools.
DICTIONARY OF CACTUS ALKALOIDS
• Anhalidine: Tetrahydroisoquinoline alkaloid (2-methyl-6,7-dimeethoxy-8-
hydroxy-1,2,3,4,-tetrahydroisoquinoline) Found in Lophophora and
• B-O-methylsynephrine: Phenolic B-phenethylamine found in citrus trees
and some cacti. No data on pharmacology, but similar compound B-Omethylepin-
ephrine produces considerable CNS stimulation.
• 3-dimethyltrichocereine: B-phenethylamine alkaloid (N,N-dimethyl-3-
hydroxy-4,5-dimethoxy-B-phenethylamine). Found in Pelecyphora and
some Trichocereus species.
• Dolichotheline: Imidazole alkaloid properly known as N-isovalerylhistamine
or 4(5)-2-N-isovalerylaminoethylimidazole. Found only in Dolichothele
and Gymnocactus species. Pharmacological action still unknown.
• Homoveratrilamine: a dimethoxy form of the mescaline molecule (3,4-
dimethoxy-B-phenethylamine). It has no activity by itself, but may alter the
mescaline experience s
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meth soft and sticky after recrystallization of the
said wannabe drug chemist.
This fact of life is due to both the nature of the product itself, and
the involved procedures required to convert ergot, morning glory
seeds, or Hawaiian baby woodrose seeds into LSD. The potency of
LSD is truly phenomenal — 10,000 doses per gram — and is easily
absorbed through the skin. This is how Albert Hofmann, the
discoverer of LSD, got his first trip. He was skilled enough that his
boo-boo involved a small enough dose that his brain was not fried.
Beginner chemists tend to get the stuff they are cooking all over
themselves, and would not be so lucky.
Lysergic acid, its precursors, and LSD are all very fragile
molecules, and quite prone to destruction by light, air and heat. The
common makeshift basement lab set-ups used by most clandestine
operators will not do for anyone contemplating LSD synthesis. Real
laboratory equipment is needed, such as a distilling kit with ground
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glass joints for doing reactions in, and for distilling home synthesized
reagents to an acceptable degree of purity. A vacuum desiccator is
essential to dry lysergic compounds without burning them. A vacuum
pump rather than an aspirator is the only acceptable source of vacuum
for this desiccator. One must be prepared to spend about $5000 up
front to equip such a lab, but the paybacks are potentially enormous if
one avoids detection. See my Third Edition of Secrets of
Methamphetamine Manufacture for many useful tips on how to obtain
chemicals and equipment, set up shop and move the product without
getting caught. The wise operator will never pass up the opportunity to
use the five-finger-discount method, industry contacts, waste
exchanges and the surplus market to stock his or her lab.
The minimum level of skill I would trust to undertake this task
would be at least a full year of college organic chemistry lab, and a
few biology courses with lab where the use of chromatography was
taught to isolate biological substances from complex mixtures. Sterile
culture technique in these biology classes is a real plus if the plan is to
cultivate ergot in a rye field. Long gone are the days when a guy like
Owsley, with only a little training and a smart wife, could buy pure
ergotamine tartarate and all the other chemicals needed to brew
legendary acids like White Lightning and Orange Sunshine. Today's
operator must be prepared to isolate lysergic acid precursors from
materials like ergot, morning glory seeds, or Hawaiian baby woodrose
seeds. He must also be ready and able to synthesize in pure form
closely watched organic reagents like diethylamine.
There is a constant and unyielding maxim in organic chemistry:
GIGO — garbage in, garbage out. If the materials used in an organic
synthesis are not pure to a reasonable degree, the result is a complex
mixture in which the desired product comprises only a small
proportion. Even a seemingly very simple reaction cannot escape this
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