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Super Instant Kava Powder (Piper methysticum)
X-pillz are the latest BZP and ephedra free legal highs that are made completely from herbal plant extracts
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Ayahuasca Medicine School lt-up pressure from the flask. If the
stirring bar bangs too violently in the flask, remove it with a magnet
rather than break the flask.
Pour the contents of the flask into a 250 ml sep funnel, and drain
the lower layer (water solution of lysergic acid hydrazide tartarate)
into a 250 ml Erlenmeyer flask wrapped in foil. To the ether layer still in
the sep funnel, add 50 ml fresh decimolar tartaric-acid solution, and
shake. Examine the water layer for the presence of lysergic acid
hydrazide with a black light. If there is a significant amount, add this
also to the Erlenmeyer flask.
Place the magnetic stirring bar in the Erlenmeyer flask, and stir it
moderately. Monitor the pH of the solution with a properly calibrated
pH meter, and slowly add .5M (20 grams per liter) sodium hydroxide
solution until the pH has risen to the range of 8-8.5. Higher pH will
cause racemization. The freebase is then extracted from the water
solution with chloroform. Two extractions with 100 ml of chloroform
should complete the extraction, but check a third extraction with the
black light to ensure that most all of the product lysergic acid
hydrazide has been extracted.
The chloroform extracts should be evaporated under a vacuum in a
500 ml flask to yield the product. This is best done by rigging the 500
ml flask for simple distillation, and applying an aspirator vacuum to
remove the chloroform. Assume that the yield from this procedure will
be about 5 grams of lysergic acid hydrazide if ergot was the crop used.
Assume that the yield will be about 7.5 grams if seeds were used.
The difference here is due to the fact that in ergot, the amides
LSD Directly From The Lysergic Amides —
The One Pot Shot
are largely composed of substances in which the portion lopped off is
about as large as the lysergic acid molecule. Seeds tend to be more
conservative as to their building upon the lysergic molecule. A careful
weighing on a sensitive scale comparing the weight of the flask before
and after would give a more exact number.
Both of these choices are really very poor, because lysergic acid
hydrazide, unlike most other lysergic compounds, crystallizes very
well with negligible loss of product. At the hydrazide stage of LSD
manufacture, one has a perfect opportunity to get an exceedingly pure
product, freed from clavine alkaloids and other garbage compounds
carried in from the extraction of the complex plant material.
I refer the reader to US patent 2,090,429 issued to Albert
Hofmann and Arthur Stoll, the dynamic duo of lysergic chemistry,
dealing with lysergic acid hydrazide. In this patent, they describe in a
rather excited state how they were able to produce pure lysergic acid
hydrazide from tank scrapings that were otherwise impure junk.
Lysergic acid hydrazide has the following properties: it dissolves
easily in acid, but is very difficultly soluble in water, ether, benzene
and chloroform. In hot absolute ethanol it is slightly school school
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ing in the cold before then adding 25 ml of diethylamine.
Stir for an additional 10 minutes, then pour the batch into a 2000
ml sep funnel. Now to the sep funnel add 800 ml of water. Mix this in
thoroughly, then add 400 ml of saturated salt solution in water. Mix
this in, then extract out the LSD by repeated extraction with 250 ml
portions of ethylene dichloride. Check with a blacklight for complete
6 LSD From Lysergic Acid And SO3
The combined ethylene dichloride extracts should be evaporated
under a vacuum as above, and the residue of LSD and iso-LSD should be
separated and treated as above.
LSD From Lysergic Acid And
LSD From Lysergic Acid
And Trifluoroacetic Anhydride
This method is a little bit lame, but it may be the method of choice if
trifluoroacetic anhydride or trifluoroacetic acid should happen to fall
from the sky into one's hands. The reason why this method is a bit lame
is threefold. Anhydrous lysergic acid is required for this reaction. To
obtain anhydrous lysergic acid, the lysergic acid hydrate yielded by the
methods in Chapter 5 must be baked under high vacuum for a
couple hours. This is obviously not good for such a delicate molecule.
The water molecule will be shed by a baking temperature of 120° C at a
vacuum of 1 mm Hg, 140° C at 2 mm Hg, and still higher
temperatures at less perfect vacuums. A MacLeod gauge is the only
instrument that I know of which is capable of accurately measuring
such high vacuums.
Another reason why this method is lacking is that the yields are
not so good as those achieved by the other synthetic routes presented in
this book. It is possible to recover the unreacted lysergic acid at the end
of the process, but this does not make up for the initial lower yield,
not to mention the added hassle of recovering and redrying the lysergic
Strike number three for this route is its propensity to give byproducts
that are difficult to separate from the desired product. I am
Practical LSD Manufacture
not talking here about the large amount of iso-LSD that this method
makes. That molecular jumbling is inconsequential, because the
lysergic acid used is itself an isomeric mixture. Rather, what can
occur here is the production of LSD and other by-products.
The mechanics of this reaction are similar to the reaction with
SOs, in that two molecules of the anhydride react with the lysergic
acid molecule to form the mixed anhydride. In this reaction, there is
no need to first react the lysergic acid with hydroxide to form the
metal salt. Also, the need to follow exact stoichiometric quantities of
reactants is not as pressing as in the SO$ method.
To do the reaction, into a 1000 ml flask (carefully dried and
equipped with a magnetic stirring bar) place 16 grams of lysergic acid
and 375 ml of acetonitrile. The lysergic acid will not dissolve. Stopper
the flask and place it in the freezer to cool the contents to -20f
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Often there are reports of blue glows and jaguars, a holy animal
in many endogenous South American cultures. I have been told that
McKenna reports that eskimos given an ayahuasca type potion
reported seeing large cats, which, of course, are not arctic
animals. I however, have found (from admittedly little reading)
McKenna's work to be questionable and less than scientific.
However, his reports often do parallel others.
MAOIs are a class of drugs that all do the same thing:
prevent the destruction of monoamines (like DMT). One MAOI is
harmaline. Harmaline is easily obtained. Syrian rue is an
excellent source. Three grams of seed, extracted with the DMT or
eaten alone should suffice. Harmaline containing plants can also
be smoked for a more rapid onset. Doses over three grams do not
add more potency. Caution should be used with MAOIs. Large doses
are hallucinogenic in and of themselves. Large doses are
unpleasant and sometimes fatal.
The remainder of this section is information cited directly
file:///C|/Documents%20and%20Settings/All%20Users/...0Culture/Ayahuasca%20and%20DMT/DMT%20FAQ%202.0.txt (3 of 13)4/14/2004 9:11:34 PM
from "Legal Highs" by Twentieth Century Alchemists. They just did
a better job than I could do. I have seen this posted around the
net and is highly recommended. This information pertains to
precautions for MAO inhibitors. READ THEM, KNOW THEM ! You will
notice several discrepancies: Legal Highs says that MAOI and
mescaline combinations are very dangerous, which contradicts
Ott's later reports on the subject. Legal Highs suggests that 5-
Me-DMT is a MAOI, which I cannot substantiate. This would render
P. tuberosa psychoactive alone. I cannot substantiate this
READ THIS!! VERY IMPORTANT. IGNORING THIS COULD LEAD TO SERIOUS
MEDICAL PROBLEMS (like death...)
Unless one is very experienced in pharmacology it is
unwise to experiment with combinations of drugs. Even when using
a single drug, thought should be given to all substances, both
food and drug, which have been taken recently. Most primitive
people fast or at least abstain from certain substances for
several days prior to taking a sacrament. Substances most
universally avoided are alcohol, coffee, meat, fat and salt. Some
drugs potentiate others. For example, atropine will increase the
potency of mescaline, harmine, cannabis and opiates. Many of the
substances discussed in this book are MAO inhibitors. MAO
(monoamine oxidase) is an enzyme produced in the body which
breaks down amines and renders them harmless and ineffective. A
MAO inhibitors interfere with the protective enzyme and leaves
the body vulnerable to these amines. A common substance such as
tyramine, which is usually metabolized with l
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@Sunday, July 22, 2018 7:49:41 PM