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or this reaction is about 25° C throughout.
When all the methyl nitrite has been bubbled into the reaction
mixture, stirring should be continued for another hour. Then, if
palladium bromide was used, it should be filtered out. Repeated
filtrations will be needed to remove all of the catalyst, because it gets
quite finely divided during the course of the reaction. This leaves a
clear light-reddish solution. If palladium bromide was used, now
adjust pH to 4-7, and allow another hour to complete the hydrolysis.
If palladium chloride or the mixed catalyst was used, these
substances are soluble in alcohol. In this case, the catalyst will be
recovered later. Here, check the pH of the solution again to be sure it is
in the proper range before proceeding.
Now the alcohol solvent must be removed. This is best done by
pouring the reaction mixture into a large filtering flask, stoppering the
top of the flask, and removing the solvent under a vacuum. Use of a
hot-water bath to speed evaporation is highly recommended for this
process. It is not OK to distill off the alcohol at normal pressure, as
the heat will cause the nitrite and NO in solution to do bad things to the
To the residue left in the flask after removal of the alcohol, add
some toluene to rinse the product out of the flask into a sep funnel.
Next, put 300 ml of water into the flask to dissolve the catalyst if
PdCla or the mixed catalyst was used. Add the water solution to the
sep funnel to dissolve carried-over catalyst there, then drain this water
12 Studies On The Production OfTMA-2
solution of catalyst into a dark bottle and store in the dark until the
next batch. If PdBr2 was used, this step can be skipped. Just store the
filtered-out PdBra under water in the dark.
Now the toluene-phenylacetone solution should be distilled
through a Claisen adapter packed with some pieces of broken glass to
effect fractionation. The first of the toluene should be distilled at
normal pressure to remove water from solution azeotropically. The
b.p. of the azeotrope is 85° C, while water-free toluene boils at 110° C.
When the water is removed from solution, turn off the heat on the
distillation, and carefully apply a vacuum to remove the remainder of
the toluene. Then with the vacuum still on, resume heating the flask,
and collect the substituted phenylacetone. Methylenedioxyphenylacetone
distills at about 140° C and 160° C using a good aspirator
with cold water. A poor vacuum source leads to much higher
distillation temps and tar formation in the distilling flask. The yield
from the reaction is close to 150 ml of phenylacetone. Its color should be
clear to a light yellow. The odor of methylenedioxyphenylacetone is
much like regular phenylacetone, with a trace of the candy shop odor
of the safrole from which it was made.
A higher-boiling phenylacetone like 2,4,5-trimethyloxyphenylacetone
is better purified as the bisulfite addition product, unless a
San Pedro Cactus (Trichocereus pachanoi)De-cored Dried Outer Skin Contact CACTUS CUZCOENSIS)RARE CUZCOENSIS)RARE SIMILAR CUZCOENSIS)RARE SKIN SKIN & CACTUS & SIMILAR and let the rice cakes slowly shift through the
fruiting temperature range. Note that everything else must be right.
The rice cake must have a fully developed mycelium network and
there must be light. The Ice-Pak should be placed between 1/4 and 1/2
inch from the rice cakes. A flat Ice-Pak will work, but if you have the
option, get one that is designed to slip into the center of a six-pak. It
will have circular indents molded into each side and it will conform to
the shape of the rice cakes better. If everything was ready, you should
see pin heads develop 3 or 4 days after you perform this adaptation. If
you don't see any develop after 3 or 4 days, you can repeat this
(26 of 39) 5/1/2002 6:54:26 PM
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 4)
operation again. The networks may not have been developed full
enough and the few days since the last attempt may have been enough
time to change this fact.
You can still initiate prolific flushes with the terrarium above the
normal temperature range. The optimum temperature for growing
mushrooms is higher than what is necessary to initiate new
mushrooms and is between 80 and 90 degrees F. This adaptation can
let the cultivator grow at the maximum rate, and still produce new
mushrooms on the cakes.
The Ice-Pak will lower the humidity in the terrarium. Mostly, this is
an issue when you have mushrooms on cakes that are part way
through the growing cycle and not ready to harvest. They will usually
survive the bad growing conditions for the six hours it takes the Ice-
Pak to initiate fruiting, but they will suffer for it. You need to have an
ultra sonic humidifier setup on your terrarium. Nothing else will be
able to keep the humidity high enough. You can turn the humidity
control up a little, but you will have to continue to adjust it down as
the Ice-Pak loses its cool. If too much moisture forms on the cakes, it
will prevent the initiation of pin heads and that was the whole purpose
of this operation.
Back to the Growing Cycle.
table of contents.
Adaptation-17: Adding Moisture to the Rice Cake.
After a cake has produced several mushrooms you can add moisture
to it. Flame sterilize a 3/16 inch drill bit. Let it cool. Use it to drill a
hole at the center of the cake. You can do this by hand. You do not
need a drill. Do not go all the way through the cake, but drill a deep
(27 of 39) 5/1/2002 6:54:26 PM
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 4)
reservoir into the cake. Cut a plastic straw to 4 inches in length. Insert
the straw 1/2 inch into the hole. The straw should fit tightly in the
cake. Straws from McDonalds are larger than most and work well.
They seal well and hold more water. Fill the straw with water daily. A
10 cc. syringe works well to fill the straws with water. You should
wait to drill the hole until the cake has produced some mushrooms
because the inside of the rice
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San Outer Cactus Pedro
Ángel Villamagua, the public prosecutor of Morona Santiago, heard the case on 22 March 2007. An arrest warrant was issued immediately against five natives, including Stalin Abrahan Tzamarenda Naichapi. By order of the judge, the police entered the first time in the homes, located Palora and captured three alleged perpetrators. In the house of Abel Luicio Naach's cousin Tzamarenda, they found a backpack brand "Quechua", which had the characteristics provided by the family when Emiliano alerted authorities about the disappearance of their son. Clothing offered during his trip to Ecuador have also been found. Those charged have been stories accusing them of murdering the Italians. A witness told the investigator that they had stayed in August huts Tzamarenda (sector Yavinza Palora) another remembered that at this time he had carried in his truck two Italian foreign, the earth terminal to Palora Puyo, where he was left to Raúl Elías Antuca, a close friend of Stalin Tzamarenda with which he organized said "shamanic tourism." Added to others, these details have led Angel Villamagua to investigate five Shuar, accused of double murder.
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