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wnward through the alumina, two zones that fluoresce blue can be spotted by illumination with a black light. The faster-moving zone contains LSD, while the slower-moving zone is iso-LSD. When the zone containing LSD reaches the spigot of the burette, it should be collected in a separate flask. About 3000 ml of the 3-1 benzene-chloroform is required to get the LSD moved down the chromatography column, and finally eluted. The iso-LSD is then flushed from the column by switching the solvent being fed into the top of the column to chloroform. This material is collected in a separate flask, and the solvent removed under a vacuum. The residue is iso-LSD, and should be stored in the freezer until conversion to LSD is undertaken. Directions for this are also given in this chapter. For the fraction containing the LSD, conversion to LSD tartrate must be done to make it water soluble, improve its keeping characteristics, and to allow crystallization. Tartaric acid has the ability to react with two molecules of LSD. Use, then, of a 50% excess of tartaric acid dictates the use of about 1 gram of tartaric acid to 3 grams of LSD. The three grams of LSD would be expected from a well-done batch out of a total 3.5 LSD/iso-LSD mix. The crystalline tartrate is made by dissolving one gram of tartaric acid in a few mis of methanol, and adding this acid solution to the benzene-chloroform elute from the chromatography column. Evaporation of the solvent to a low volume under a vacuum gives crystalline LSD tartrate. Crystals are often difficult to obtain. Instead, an oil may result due to the presence of impurities. This is not cause for alarm; the oil is still likely 90%+ pure. It should be bottled up in dark glass, preferably under a nitrogen atmosphere, and kept in a freezer until moved. If chromatography reveals that one's chosen cooking method produces little of the iso products, then the production of the tartrate salt and crystallization is simplified. The residue obtained at the end Practical LSD Manufacture 32 of the batch is dissolved in a minimum amount of methanol. To this is then added tartaric acid. The same amount is added as above: one gram tartaric acid to three grams LSD. Next, ether is slowly added with vigorous stirring until a precipitate begins to form. The stoppered flask is then put in the freezer overnight to complete the precipitation. After filtering or centrifuging to isolate the product, it is transferred to a dark bottle, preferably under nitrogen, and kept in the freezer until moved. LSD from (so-LSD Two variations on this procedure will be presented here. The first is the method of Smith and Timmis from The Journal of the Chemistry Society Volume 139, H pages 1168-1169 (1936). The other is found in US patent 2,736,728. Both use the action of a strong hydroxide solution to convert iso material into a mixture that contains active and iso material. At equilibrium, the mixture contains about 2/3 % Pure Lagochilin Ayahuasca Black Negra San Pedro Cactus Trichocereus vine vine ydrolysed ergot alkaloids, to unreacted lysergic acid, or lysergic acid hydrazides to iso- LSD and God knows what substances created by the mishandling of the raw materials and product, a contaminated product is much easier to make than a pure one. The use of large volumes of solvents poses twin problems: obtaining them and disposing of them. Both problems are made vastly Practical LSD Manufacture 70 simpler by recycling the solvents. Just because a solvent has been used once in a given stage of the process does not mean its useful lifetime is over. For example, the solvent used for defatting the crop is easily made as good as new by distilling it to free it of its load of fat. Other solvents are not so easily recovered for re-use because the procedure calls for the given solvent to be removed from the product by vacuum evaporation. In this case, the solvent can be collected in a cold trap placed along the vacuum line on its way to the vacuum source. If a pump is used to create the vacuum, such a trap is vital to prevent solvent vapors from getting into the pump oil, thereby ruining the lubrication and the vacuum created. A cold trap can be constructed of either glass or steel; it need only be large enough to hold the solvent collected, and airtight so as not to ruin the vacuum with leaks. This cold trap is then cooled down with dry ice during vacuum evaporations to condense the solvent vapors in the trap. The solvent recovered in the trap can be re-used in the given stage of the process from whence it came. I would not co-mingle recovered solvents from different stages. For example, chloroform from the alkaloid extraction of the crops should be kept for that usage, and not be used for LSD crystallization, because it will also contain some ammonia and methanol. The recovery of ether, for example, from method 2 of lysergic acid production, poses a special problem. This problem is the formation of explosive peroxides in ether during storage. Ether containing water and alcohol, as would be the case for this recovered solvent, does not form much peroxide. There is a possibility that dry ether can be made free of peroxides by shaking the ether with some 5% ferrous sulfate (FeSO4) solution in water prior to distilling. Failure to do this may expose the operator to a fiery explosion during distillation. Ice water flowing through the condenser, and an ice-chilled receiving flask, are required to get an efficient condensation of the ether during distillation. 11 Keeping Out Of Trouble 71 II Keeping Out Of Trouble The dangers of LSD manufacturing do not end with the possibility that the cooker may spill some of the stuff on himself and fry his brain. There is a much more malignant danger facing those who embark upon this course: Johnny Law. The conduit through which those shit-eating dogs travel to get to you is your associates. If you are cooking alone with no partners in crime, your safety has been impro Premium Mimosa Hostilis Root Bark Ayahuasca Black Negra San Pedro Cactus Trichocereus Ayahuasca Retreat

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