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The scale used to portion out Practical LSD Manufacture 52 the ingredients for this synthesis should at least be a very sensitive triple-beamer, and its accuracy should be checked using new corrosion-free brass weight standards. Atmospheric humidity is a very real threat. NaOH, KOH, and lysergic acid will all pull water from the air. This not only makes accurate weighing impossible, but it also introduces water to the batch. For this reason, air conditioning or the dry indoor heat of winter are best during the unavoidable handling and weighing of reagents. Two methods will be presented here, the first being the specific synthetic method for LSD given in example ten of US Patent 2,774,763. The other is the general method given in Journal of Organic Chemistry Volume 24, pages 368 to 372. Both are authored by William Garbrecht, a true hero of LSD synthesis. The patent dates from 1955, while the Journal article dates from 1958.1 leave it to the serious experimenter to decide which is more advanced. No doubt, both are operable. Patent Method 15 grams of lysergic acid is quickly weighed out, and placed in a dried 1000 ml flask equipped with a magnetic stirring bar. 200 ml of methanol is added to dissolve the acid, then the flask is stoppered while either 2.22 grams lithium hydroxide hydrate, or 2.09 grams sodium hydroxide pellets or 2.94 grams KOH pellets is weighed out and dissolved in 200 ml methanol. The use of lithium hydroxide is preferred because it doesn't absorb water from the air, thereby messing up the weighing. Lithium hydroxide, on the other hand, is not a very common item, and will raise red flags that attract unwelcome attention. NaOH and KOH, however, are very mundane items. Further, a freshly opened bottle containing them can safely be assumed to be free of water. Quick weighing under low humidity will not add appreciable amounts of water to it. If the choice was mine to make, I would use NaOH or KOH. 6 LSD From Lysergic Acid And SO3 53 The LiOH or NaOH or KOH solution is now added to the methanol solution containing lysergic acid. After a period of stirring to assure complete reaction to the metal salt of lysergic acid, the solvent is distilled off under a vacuum, leaving a bubbly residue clinging to the glass at the bottom of the flask. If the lysergic acid is pure, such as that made by method 2 in Chapter 5, this residue will have a glassy appearance. No heat stronger than steam or hot water should be used to drive the distillation. The residue in the flask still contains traces of water and methanol. The water comes from the reaction of the hydroxide with the acid, and from the lithium hydroxide, if that was used. 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